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Methods: Potentiometric nonaqueous titrations(potentionmetry) and nonaqueous titrations of malachite green indicator(indicator method) were adopt. 方法:採用非水電位滴定法(以下簡稱電位法)和以孔雀綠爲(wèi)指示劑的非水滴定法(以下簡稱指示劑法)。